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Methaqualone
I though phenol was air/uv sensitive with respect to polymerization?
18-1-2021 at 07:52
by: njl
Silane as a reducing agent
Silane gas can be readily generated from silicide salts (Mg2Si for example). [b]Substituted[/b] sila ...
17-1-2021 at 16:28
by: njl
Synthesis section?
I like the idea of a "Rhodium for chemistry in general". organic-chemistry.org is similar but I thin ...
17-1-2021 at 16:20
by: njl
How to calcine aluminum but not copper.
I am beginning to think you are being intentionally dense. If the very DEFINITION of a word doesn't ...
17-1-2021 at 06:06
by: njl
How to calcine aluminum but not copper.
"Calcine" has a very specific meaning to me (and probably a majority of the people here). Whatever t ...
16-1-2021 at 11:35
by: njl
Nitromethane from Nitromethane/Oil
Nitromethane is slightly soluble in water. If enough is pulled out of the oil, it could coalesce int ...
15-1-2021 at 09:59
by: njl
Nitromethane from Nitromethane/Oil
If you could get more information on the type of oil that would make separation easier. If the oil i ...
15-1-2021 at 09:33
by: njl
1,3,5-trichlorohexahydrotriazine
As mentioned above, the electrophilic Cl+ is needed for this reaction. I'm guessing NaDCC is less la ...
15-1-2021 at 08:10
by: njl
Carbonate ester synthesis from urea?
As discussed in other threads, simple carbonate esters can be made simply from the alcohol and urea ...
15-1-2021 at 07:16
by: njl
How to calcine aluminum but not copper.
I have never seen "calcine" refer to that process, nor can I find any info on anything under that na ...
14-1-2021 at 16:22
by: njl
How to calcine aluminum but not copper.
Could you by any chance mean chlorinate and not calcine?
14-1-2021 at 07:16
by: njl
Rice husk ash, an amazing material and its uses!
If rice husks are 20 percent silica by dry mass, how can they be turned into effective charcoal? Isn ...
12-1-2021 at 07:14
by: njl
Peracetic acid
Yes and yes. Peracids can be used as selective oxidizing agents for the formation of epoxides, ester ...
12-1-2021 at 06:59
by: njl
Synthesis of N,N'-dialkyloxamides
Relevant paper: https://doi.org/10.1016/j.cclet.2018.01.003
And abstract: https://www.sciencedirect ...
11-1-2021 at 09:40
by: njl
Friedel-Crafts acylation of anilides
Note 1 in the following:


http://www.orgsyn.org/demo.aspx?prep=cv3p0191
11-1-2021 at 09:26
by: njl
Trying to get rid of chemicals. Nearish Philadelphia
Missed the deal of a lifetime :(
9-1-2021 at 16:13
by: njl
Friedel-Crafts acylation of anilides
Amines are lewis bases while AlCl3 is a lewis acid. So there will probably be some reaction there, m ...
9-1-2021 at 10:21
by: njl
Chlorination
In Shulgin's report on the chlorination of 2C-H to 2C-C, he uses liquid chlorine as a reagent. Why c ...
8-1-2021 at 15:29
by: njl
Successful Synthesis of 1-Amino-3-nitroguanidine Nitrate
Impressive stuff! Will you be posting a write up on this synth?
8-1-2021 at 07:07
by: njl
hydrobenzamide from benzaldehyde and ammonia
Excellent write up!
7-1-2021 at 06:10
by: njl
ETN question
I believe phosphoric acid also works as an acid catalyst. As far as I know, an acid is needed to pro ...
5-1-2021 at 11:02
by: njl
ETN question
Using HNO3/H2SO4 is generally preferable to (X)NO3/H2SO4, but in both cases sulfuric acid is needed. ...
5-1-2021 at 10:33
by: njl
ETN question
At least using acetone you can leave behind most of the solids. I don't think the idea was to pull o ...
5-1-2021 at 10:10
by: njl
Freestyle chem
I very much enjoy "freestyle" chemistry, just winging a procedure based on background knowledge. For ...
5-1-2021 at 07:22
by: njl
ETN question
How dry is your reaction mixture? Even though part of the reaction is dehydration, I believe you do ...
5-1-2021 at 07:01
by: njl
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