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Methylene Dithiocyanate preparation
See the paper:
13-8-2015 at 07:16
by: organichem
Experimental: Alternative to Al/Hg - the Al/Cu
In-situ reduction of ketone/nitroalkane didn't work for me - I only got aminoalkane
Perhaps with pr ...
13-9-2014 at 09:32
by: organichem
Chloroacetic Acid from TCCA and S/I2 Catalyst?
Well - I'm interested in the TCCA method and was asking myself as I read through the paper:

[quot ...
31-7-2014 at 23:26
by: organichem
New benzofuran compound
Currently I'm working on different things;
1) more convenient route to 2,3,6,7-tetrahydrobenzodifur ...
14-7-2014 at 23:31
by: organichem
Reductive amination
I tried a reductive Al/Cu amination like Al/Hg with a ketone and nitromethane at 25 mmol scale but r ...
15-5-2014 at 04:49
by: organichem
Butyllithium
Harzard notes are substantial for BuLi - but I'm used to work with the Schlenk-technique and with py ...
29-4-2014 at 04:17
by: organichem
Butyllithium
Hey folks, I want to prepare some BuLi - preferably in cyclohexane.

I've read several papers deal ...
28-4-2014 at 02:36
by: organichem
Preperation of Zinc Amalgam?
What do you think of the reduction via tosylhydrazone?
[url=http://www.orgsyn.org/demo.aspx?prep=cv ...
27-4-2014 at 11:32
by: organichem
Odd lettering in IUPAC name
That's a kind of nomenclature for stereoisomers where the configuration is decribed with the
aid of ...
13-3-2014 at 22:20
by: organichem
How to separate iron oxalate and manganese oxalate
Fe ions are only soluble in acidic oxalate solutions. Mn ions seem to act in a similar way,
so you ...
8-2-2014 at 01:35
by: organichem
4-alkylthio-2,5-dimethoxybenzaldehyde, Sulfuric Duff reaction
What do you think on another substrate... at the moment I'm searching for an more-or-less OTC proced ...
10-1-2014 at 02:18
by: organichem
Nitroalkane syntheses ?
A maybe interesting article I found:
[url=http://pubs.rsc.org/en/Content/ArticleLanding/2008/GC/B80 ...
20-11-2013 at 07:25
by: organichem
Need help about Nitrostyrene synthesis
Small-scale trial of the Henry-Reaction with 2-HEAF (~10 mmol)

1.3 g anisaldehyde (MW 136, ~9.6 m ...
18-11-2013 at 00:01
by: organichem
Need help about Nitrostyrene synthesis
I was curious if it would work and tried the HEAF-method on a 10 mmol-scale, using anisaldehyde and ...
16-11-2013 at 03:52
by: organichem
Need help about Nitrostyrene synthesis
Well, I found a very interesting/promising article - but I've no access to it:
[url=http://pubs.acs ...
14-11-2013 at 05:54
by: organichem
Preparation of gentisaldehyde
Yeah, Nicodem - sadly I'm not the person who has access to such things like BBr[sub]3[/sub]...
I go ...
29-9-2013 at 05:28
by: organichem
Preparation of gentisaldehyde
Thanks, Nicodem for the papers, I'll get a look on them next week.

Well I just thought it would b ...
22-9-2013 at 06:36
by: organichem
Preparation of gentisaldehyde
Hi folks,

I'm new here at the SMDB, I've been reading quite a while and decided to register final ...
18-9-2013 at 02:21
by: organichem

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