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Purification of Toluene
After a few failed MPVO runs I tested my Ace brand toluene (which I had previously just dried over C ...
20-9-2012 at 16:51
by: scientician
Simple(er)Aluminum Isopropoxide prep experiment for later this week.
Following up on this old post - a very small amount of gallistan (gallium tin alloy) worked brillian ...
29-5-2012 at 01:06
by: scientician
Prep. of dilute sodium isopropoxide from NaOH
Vogel confirms this actually works. :D
26-2-2012 at 15:31
by: scientician
testosterone from cholesterol
Sorry to necro this thread. I know a great deal about steroid chemistry and need to feel important. ...
26-2-2012 at 00:35
by: scientician
Benzaldehyde from phenylalanine
If you can't explain it simply, you don't understand it well enough.

Say what you will, but my se ...
24-2-2012 at 20:20
by: scientician
Benzaldehyde from phenylalanine
Carbon #8 on this badboy is the chiral one. If you oxidize it to the aldehyde, the chirality of the ...
24-2-2012 at 17:48
by: scientician
Prep. of dilute sodium isopropoxide from NaOH
An experiment I'd like to perform calls for a very dilute solution (0.07M) of sodium isopropoxide in ...
24-2-2012 at 16:21
by: scientician
Calcium pyruvate to sodium pyruvate or pyruvic acid
I do this all the time, (oxalic acid and aq. calcium pyruvate.) It does work quite well, but I tend ...
29-10-2011 at 04:19
by: scientician
Chemicals For Sale
So, I see you're an aficionado of the "groovy-groovy sherm." Let me tell you young man, it may be ...
29-10-2011 at 04:07
by: scientician
DIY magic filter papers - a video demonstration
Sorry to keep digging this old shit up. I worked on this last night, both with a 25% solution of wa ...
15-5-2011 at 11:32
by: scientician
Replacement of GAA in bleach oxidations
Did my reaction, and near as I can tell without NMR analysis, it worked. No tar formed, and I have ...
3-5-2011 at 21:47
by: scientician
I'll pay you to come up with a synthesis for me.
If the prospect of using HCl in the gaseous phase has you concerned, let me assure you that glycine ...
29-4-2011 at 01:42
by: scientician
I'll pay you to come up with a synthesis for me.
Yo, I'm with Mr. Crow. I think you should learn all the tedious bits yourself. You might find you ...
29-4-2011 at 01:10
by: scientician
Boiling Flask Integrity
Bubbles aren't ideal, but they're not what you need to be worried about. Look instead for cracks, e ...
25-4-2011 at 20:15
by: scientician
Replacement of GAA in bleach oxidations
Wow, this is a really old thread! :P Sorry for the resurrection; I have full online journal article ...
25-4-2011 at 13:40
by: scientician
Simple(er)Aluminum Isopropoxide prep experiment for later this week.
Interesting. Since both the reagents are solids at STP, it could feasibly be reacted solvent free. ...
19-12-2010 at 22:31
by: scientician
Simple(er)Aluminum Isopropoxide prep experiment for later this week.
I am seeking comments on a a simple experiment I have underway to see if Aluminum isopropoxide can b ...
19-12-2010 at 17:51
by: scientician
Separation of isoflavinoids
I'm assuming simple paper chromatography just wont do?

I sneaked a peek at equol, as well as th ...
15-12-2010 at 02:03
by: scientician
Bio-stoichiometry & baker's yeast question
It has recently been brought to my attention that baker's yeast can be made to produce alcohols from ...
15-12-2010 at 01:41
by: scientician

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