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Total synthesis of muscimol + extraction and isolation from Amanita muscaria Fantastic Write up!
Can't remember the last time I heard of someone using a reactive Borane comp ... |
23-12-2024 at 11:00 by: walruslover69 |
Phthalimide -> Anthranillic acid Reaction Not Working There is also a route to anthranilic acid from Methyl Anthranilate, sold as bird repellent or grape ... |
7-12-2024 at 11:21 by: walruslover69 |
Glass Batch Reactors vs RBFs The only time I have seen option 2 used was for the short path distillation of cannabinoids. Heating ... |
24-11-2024 at 15:39 by: walruslover69 |
Glass Batch Reactors vs RBFs I have actually just been scaling up a reaction from a 10l flanged round bottom flask to a 50L jacke ... |
22-11-2024 at 14:11 by: walruslover69 |
THC Reclaim Chemistry There is a lot of interesting chemistry with cannabinoids, main problem with trying to investigate h ... |
29-10-2024 at 12:38 by: walruslover69 |
Interaction between NaBH4 and CuCN in acetonitrile-water? This would be very interesting if feasible. The only reservation I might have is the copper nanopart ... |
23-9-2024 at 12:56 by: walruslover69 |
Subcritical Water Reactor (asking for experience) I am very interested recently in green chemistry, specifically replacing organic solvents with subcr ... |
9-8-2024 at 18:06 by: walruslover69 |
KCl + Ca does release K metal, but KCl + Mg not ? I calculated
2KCl+Ca→2K+CaCl2 ΔG=0 at 1085K
2KCl+Mg→2K+MgCl2 ΔG=0 at 1523K
3KCl+Alâ ... |
6-8-2024 at 12:33 by: walruslover69 |
Acrylic acid by dehydration of Lactic acid? From my brief reading this doesn't seem to be reasonably feasible on the small scale. This paper out ... |
2-8-2024 at 05:18 by: walruslover69 |
Hückel method for Vinylamine and others I'm sure there is a way to calculate vinylamine with the Huckel method, but it would not be as simpl ... |
23-7-2024 at 04:09 by: walruslover69 |
Separating Toluene from N-Butyl Acetate yes |
28-6-2024 at 11:24 by: walruslover69 |
Does anyone do phosphorescent experiments in sealed glass containers? doped Zinc sulfide, Calcium Sulfide, Strontium aluminate. There are also lot's of naturally occurrin ... |
18-6-2024 at 14:47 by: walruslover69 |
Vacuum regulation @Sulaiman I wish I had an old picture to show, the whole system was insane. For some background This ... |
12-6-2024 at 05:37 by: walruslover69 |
Vacuum regulation My old lab used to have a comically oversized rotary vane pump connected to our rotary evaporator. W ... |
11-6-2024 at 06:56 by: walruslover69 |
Does anyone do phosphorescent experiments in sealed glass containers? There are probably very few compounds that phosphoresce at 0C but not 25C, just because it's such a ... |
30-5-2024 at 11:30 by: walruslover69 |
Does anyone do phosphorescent experiments in sealed glass containers? Any excuse to work with liquid nitrogen is always a good one!
When cooled down to liquid nitroge ... |
30-5-2024 at 06:09 by: walruslover69 |
Does anyone do phosphorescent experiments in sealed glass containers? We used special cuvettes similar to this. https://www.amazon.com/Fluorescence-Cuvette-Spectrophotome ... |
29-5-2024 at 08:22 by: walruslover69 |
Does anyone do phosphorescent experiments in sealed glass containers? Yes. I did some academic research on organic phosphorescence and it's very common to measure with an ... |
28-5-2024 at 07:14 by: walruslover69 |
preparation of tryptophol by baker's yeast fermentation of L-tryptophan That's Fantastic Work. Great Job! You were very thorough it seems with the TLC. Does this reaction o ... |
28-3-2024 at 12:53 by: walruslover69 |
Tryptophan decarboxylation improved Read my thread on an improved synthesis/purification
as dicyanin stated, forming the benzoic aci ... |
12-3-2024 at 09:22 by: walruslover69 |
Metallic soaps Once upon a time, I was synthesizing some CdSe quantum dots at university. We would mix Cadmium oxid ... |
6-3-2024 at 10:08 by: walruslover69 |
Sulfuric Acid photoluminescence. I have synthesized fluorescent carbon nanoparticles by simply heating organic compounds in sulfuric ... |
15-2-2024 at 13:02 by: walruslover69 |
Reduction of Nitro > Amine: Sodium Aluminum Hydride (NaAlH4)/Lithium Borohydride (LiBH4)? I have tried several reduction reactions of nitro compounds into amines with both LiAlH4 and NaBH4. ... |
15-1-2024 at 17:36 by: walruslover69 |
Phosphorescence from boric acid + salicylic acid I worked on Phosphorescence during my PhD research. I spent close to 2 months making boron carbon ni ... |
25-12-2023 at 15:20 by: walruslover69 |
Synthesis of iron(III)-acetylacetonate Fun complex! We synthesized this as well as the copper and cobalt compelx in my undergrad inorganic ... |
7-12-2023 at 14:12 by: walruslover69 |
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