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Total synthesis of muscimol + extraction and isolation from Amanita muscaria
Fantastic Write up!

Can't remember the last time I heard of someone using a reactive Borane comp ...
23-12-2024 at 11:00
by: walruslover69
Phthalimide -> Anthranillic acid Reaction Not Working
There is also a route to anthranilic acid from Methyl Anthranilate, sold as bird repellent or grape ...
7-12-2024 at 11:21
by: walruslover69
Glass Batch Reactors vs RBFs
The only time I have seen option 2 used was for the short path distillation of cannabinoids. Heating ...
24-11-2024 at 15:39
by: walruslover69
Glass Batch Reactors vs RBFs
I have actually just been scaling up a reaction from a 10l flanged round bottom flask to a 50L jacke ...
22-11-2024 at 14:11
by: walruslover69
THC Reclaim Chemistry
There is a lot of interesting chemistry with cannabinoids, main problem with trying to investigate h ...
29-10-2024 at 12:38
by: walruslover69
Interaction between NaBH4 and CuCN in acetonitrile-water?
This would be very interesting if feasible. The only reservation I might have is the copper nanopart ...
23-9-2024 at 12:56
by: walruslover69
Subcritical Water Reactor (asking for experience)
I am very interested recently in green chemistry, specifically replacing organic solvents with subcr ...
9-8-2024 at 18:06
by: walruslover69
KCl + Ca does release K metal, but KCl + Mg not ?
I calculated

2KCl+Ca→2K+CaCl2 ΔG=0 at 1085K

2KCl+Mg→2K+MgCl2 ΔG=0 at 1523K

3KCl+Alâ ...
6-8-2024 at 12:33
by: walruslover69
Acrylic acid by dehydration of Lactic acid?
From my brief reading this doesn't seem to be reasonably feasible on the small scale. This paper out ...
2-8-2024 at 05:18
by: walruslover69
Hückel method for Vinylamine and others
I'm sure there is a way to calculate vinylamine with the Huckel method, but it would not be as simpl ...
23-7-2024 at 04:09
by: walruslover69
Separating Toluene from N-Butyl Acetate
yes
28-6-2024 at 11:24
by: walruslover69
Does anyone do phosphorescent experiments in sealed glass containers?
doped Zinc sulfide, Calcium Sulfide, Strontium aluminate. There are also lot's of naturally occurrin ...
18-6-2024 at 14:47
by: walruslover69
Vacuum regulation
@Sulaiman I wish I had an old picture to show, the whole system was insane. For some background This ...
12-6-2024 at 05:37
by: walruslover69
Vacuum regulation
My old lab used to have a comically oversized rotary vane pump connected to our rotary evaporator. W ...
11-6-2024 at 06:56
by: walruslover69
Does anyone do phosphorescent experiments in sealed glass containers?
There are probably very few compounds that phosphoresce at 0C but not 25C, just because it's such a ...
30-5-2024 at 11:30
by: walruslover69
Does anyone do phosphorescent experiments in sealed glass containers?
Any excuse to work with liquid nitrogen is always a good one!

When cooled down to liquid nitroge ...
30-5-2024 at 06:09
by: walruslover69
Does anyone do phosphorescent experiments in sealed glass containers?
We used special cuvettes similar to this. https://www.amazon.com/Fluorescence-Cuvette-Spectrophotome ...
29-5-2024 at 08:22
by: walruslover69
Does anyone do phosphorescent experiments in sealed glass containers?
Yes. I did some academic research on organic phosphorescence and it's very common to measure with an ...
28-5-2024 at 07:14
by: walruslover69
preparation of tryptophol by baker's yeast fermentation of L-tryptophan
That's Fantastic Work. Great Job! You were very thorough it seems with the TLC. Does this reaction o ...
28-3-2024 at 12:53
by: walruslover69
Tryptophan decarboxylation improved
Read my thread on an improved synthesis/purification

as dicyanin stated, forming the benzoic aci ...
12-3-2024 at 09:22
by: walruslover69
Metallic soaps
Once upon a time, I was synthesizing some CdSe quantum dots at university. We would mix Cadmium oxid ...
6-3-2024 at 10:08
by: walruslover69
Sulfuric Acid photoluminescence.
I have synthesized fluorescent carbon nanoparticles by simply heating organic compounds in sulfuric ...
15-2-2024 at 13:02
by: walruslover69
Reduction of Nitro > Amine: Sodium Aluminum Hydride (NaAlH4)/Lithium Borohydride (LiBH4)?
I have tried several reduction reactions of nitro compounds into amines with both LiAlH4 and NaBH4. ...
15-1-2024 at 17:36
by: walruslover69
Phosphorescence from boric acid + salicylic acid
I worked on Phosphorescence during my PhD research. I spent close to 2 months making boron carbon ni ...
25-12-2023 at 15:20
by: walruslover69
Synthesis of iron(III)-acetylacetonate
Fun complex! We synthesized this as well as the copper and cobalt compelx in my undergrad inorganic ...
7-12-2023 at 14:12
by: walruslover69
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