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Chlorinating Carboxylic Acids
I don't know what products you are interested in producing.
But, Phosphorus Oxychloride can be pr ... |
30-1-2025 at 17:30
by: zed |
Sassafras oil long term storage
UMMM. Without a license, access to this reagent is relatively difficult.
If you reside in the w ... |
2-12-2024 at 16:36
by: zed |
Making Magnesium Turnings
On the other hand, as I recall, older air-cooled VW engine blocks were made of Magnesium. Throw a r ... |
16-11-2024 at 17:11
by: zed |
Dichromate Synthesis from Chromium metal and NaClO3
I'm a man, but I can probably change, if I really have to.... I guess.
On a practical note. Re ... |
16-11-2024 at 17:03
by: zed |
Should I buy this furnace on ebay?
I am proud to say that I improvised my own furnace. I needed to de-temper a cast metal weight lifti ... |
5-7-2024 at 16:33
by: zed |
Scaleup woes - Reduction of Nitrostyrenes to Nitroalkanes
Reduction of Nitrostyrenes?
Catalytic Hydrogenation, via Platinum Black, in an Acetic environment ... |
5-7-2024 at 16:03
by: zed |
Extracting the alkaloid scopolamine from datura stramonium seeds?
Nightshade is a common weed here in Oregon. I do not recommend experimenting with Nightshade Alkalo ... |
2-7-2024 at 16:38
by: zed |
Organic carbon?
OK guys, fun is fun. And, Organic Carbon is Charcoal. It is a powerful reducing agent.
Very use ... |
6-5-2024 at 16:45
by: zed |
Recrystallization and stirring
Ummm. Back when we rode around on dinosaurs, I once crystalized a nitro-olefin via rapid stirring.
... |
20-3-2024 at 17:31
by: zed |
Stainless Steel Reaction Vessels
Umm. Decarboxylation of Sodium Benzoate? Guys often use "tin" cans for this type reaction. Cheap ... |
20-3-2024 at 17:15
by: zed |
Nitroethane synthesis trouble
Nitroethane is tough to make. Unfortunately, here in the USA, its sale is restricted.
Some of th ... |
5-1-2024 at 16:22
by: zed |
Is LiH a strong enough base to deprotonate indole
Acetic Anhydride might not be a good choice to protect Indolic Nitrogen. In general, it is not wild ... |
6-9-2023 at 17:31
by: zed |
Alcohol burner usefulness? Also, some glassware heating questions.
I don't generally use 'em, but they have their uses. The spirit lamp, used in conjunction with a bl ... |
15-7-2022 at 23:23
by: zed |
Benzene to benzaldehyde conversion
Lots of better ways to make Benzaldehyde. Oxidation of Benzyl Alcohol or Chlorination of Toluene, ... |
15-7-2022 at 02:36
by: zed |
Drying an impossibly deliquescent iminium salt (how stable are iminium salts?)
Ummm. I like to use 100% Ethanol as a desiccant. Just add it to your soupy-salt, and distill off s ... |
15-7-2022 at 02:15
by: zed |
Homemade and Repurposed Lab Gear
Ummm. My Ringstands finally got built.
Ten pound, Cast iron, weight plates, strongly resisted be ... |
14-7-2022 at 21:06
by: zed |
Value of gold
Easy enough to make those fancy heavy elements. Just bang a couple of Neutron Stars together, and c ... |
16-6-2022 at 07:35
by: zed |
Clandestine Chemistry Series
This is a chemistry site, not a drug site.
Various drug synthesis questions are discussed here, b ... |
16-6-2022 at 06:12
by: zed |
2,5-dimethoxybenzaldehyde question
Easy enough to find out. Try it. |
16-6-2022 at 05:53
by: zed |
Trinitrotriamminecobalt - Co(NH3)3(NO2)3
Ummm. Should this be posted in "Energetic Materials"?
Seems to me, that a similar material, seve ... |
3-6-2022 at 00:31
by: zed |
LAH Reduction
Now, chemrox! You know perfectly well, that mailing LiALH4... is against postal regulations! |
8-5-2022 at 00:20
by: zed |
Some practical questions about Grignard reactions
To my recollection, this type synthesis calls for an addition of the Grignard Reagent to the Nitrile ... |
7-5-2022 at 05:24
by: zed |
LAH Reduction
Ummm. Blew an addition funnel out of. a flask?
I had a buddy that blew apart a building perfor ... |
26-4-2022 at 22:08
by: zed |
Can Platinum be used as a hydrogenation catalyst?
In my youth, Platinum was about $300/ Oz.. Palladium was $30-$40/ per Oz..
Gold could be purchas ... |
22-4-2022 at 05:31
by: zed |
Make Phosphorus from Ca phosphate and Mg powder ?
This is unlikely to produce elemental Phosphorus.
But, if it actually does.... Please post in th ... |
15-4-2022 at 02:07
by: zed |
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