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Alcl3 by double displacement?
I've recently been looking for an easy way to get aluminium chloride, and I came up with this idea. ... |
19-11-2022 at 03:42
by: sceptic |
Hydrothermal synthesis of rubies from chromium-doped Alcl3.6H2O
I've had a mixture of Alcl3.6H2O, spiked with CrCl3 hydrate, sealed into a vial of borosilicate glass. I'm going to grill ... |
14-11-2021 at 16:34
by: Admagistr |
More thoughts (rants) on Alcl3 Chlorination of alcohols
So I did more thinking since my previous post about why Alcl3 doesn't work for chlorinating aliphatic alcohols and this is what I came
up with as potential ... |
8-12-2020 at 20:43
by: EverythingAl2O3 |
Alcl3 is an alternative to SOCl2
... ks but is the only option.
So I thought about the mechanisms of how they work, and realized that Alcl3 works in a very similar way in Friedel-Crafts alkylation. So
I came up with the mechanism atta ... |
3-12-2020 at 18:12
by: EverythingAl2O3 |
Anhydrous Alcl3 from Dean-Stark apparatus?
I'm pretty new to using dean-stark traps, and I'm wondering, could a toluene-water (or similar) immi ... |
9-11-2020 at 10:22
by: p4rtridg3 |
ZnCl2 + Al -> Alcl3 troubles... again
... onnected to a 100mm U pipe that fed straight into a hdpe bottle. Also, in an attempt to contain the Alcl3 I used parafilm to seal the
bottle and the U pipe.
This time around I used an excess of 50 ... |
9-7-2020 at 21:20
by: Opylation |
ZnCl2 + Al -> Alcl3
So I’m posting this right after I attempted a synth of Alcl3 that I was a little less than prepared for. So I’m posting to see if
anyone else has perform ... |
22-6-2020 at 00:36
by: Opylation |
Using CHCl3 as a solvent for the capture of Alcl3
... o everybody,
I am curious as to what you guys think about using CHCl3 as a solvent for capturing Alcl3 sublimate? I found the easiest way to go about
making Alcl3 for me was to first make CuCl2, de ... |
30-5-2020 at 21:18
by: Opylation |
Anhydrous Alcl3
I need some anhydrous Alcl3. I have two options:
1. Make it from Alcl3.6H2O.
2. Make it from ZnCl2.
I don't know ho t ... |
27-7-2019 at 08:52
by: Paul St. Germain |
Group buys for anhydrous Alcl3, dibromomethane, n-bromobutane, TEMPO
... ar that much. It's separate from everything else though, and optional.
For the other reagents, (Alcl3, CH2Br2, BuBr) I can do $15/100g or $30/250g plus shipping. I don't believe I'd be able to sh ... |
5-11-2018 at 02:50
by: Melgar |
extracting Alcl3 from aq using organic solvent?
Alcl3 anhydrous is soluble in CCl4, CHCl3 according to wiki hence I speculate it should also be solu ... |
23-5-2018 at 16:31
by: fusso |
Alcl3 from HCl and foil
... enerator.
Anyway, my plan is to mix aluminum foil with muriatic acid. Using:
6 HCl + 2 Al = 2 Alcl3 + 3 H2
I'm not 100% sure, but from a bit of googling, I found that muriatic acid is about 1 ... |
4-3-2018 at 20:58
by: zenmanenergy |
anhydrous Alcl3 with cucl2 ?
i need to know where cupperchloride dissolves in to form anhydrous
Alcl3. If i have absolute ethanol and react some aluminium with cucl2 and than remove the ethanol by ... |
26-11-2017 at 13:13
by: Mn2Dc |
feasibility of forming the Alcl3 complex with methyl chloride and phosphorus trichloride
... s trichloride aluminum chloride mixture to overhead stirring for 24 hours to break up clumps of the Alcl3.
Then I put the mixture under magnetic stirring and in time much but not all of the mixture s ... |
27-8-2016 at 12:04
by: obeliscus |
Anhydrous Alcl3 from ZnCl2
... ime tweaking and have figured out a way of using what equipment i have and can boast a 40% yield of Alcl3 using the Zinc Chloride and
aluminium powder reaction. And it's decent quality - works a treat ... |
19-6-2015 at 10:11
by: ChemPlayer |
Difficulty with Alcl3/Urea DES
I am trying to create an Aluminum Chloride/Urea deep eutectic solvent. This and the other type IV DE ... |
21-4-2015 at 14:13
by: nlegaux |
LAH from LiH and Alcl3
... t prepared from the reaction between lithium hydride (LiH) and aluminium chloride:[2][3]
4 LiH + Alcl3 → LiAlH4 + 3 LiCl"
For the purposes of another experiment I need a very small quantity of ... |
28-12-2014 at 10:16
by: nickec |
Chlorothermal reactions (chloride thermites) for preparing Alcl3 and KAlCl4
WARNING: This is a hypothetical thread of untested and potentially highly dangerous thermite-like re ... |
17-4-2014 at 02:04
by: deltaH |
Potential Anhydrous Alcl3 Synthesis
... n the bottom of the RBF. From my research it seems like a viable method of producing the invaluable Alcl3. I will hopefully be giving it
a go in the near future. |
15-2-2014 at 20:49
by: thebean |
Anhydrous Alcl3 handling and storage
Some issues with anhydrous Alcl3 ( I have recently received 500 g I have just purchased ) :
It arrived in a cardboard box, ... |
18-4-2012 at 14:35
by: xwinorb |
Alternate route of Alcl3 synthesis
Today, it seems that I might have found an alternate (though more complex) route of anhydrous Alcl3 synthesis that doesn't involve high
temperatures (not quite) or corrosive gases.
Firstly, s ... |
8-4-2012 at 03:39
by: weiming1998 |
How to make relatively pure Alcl3
Hello,
I want to make relatively pure Alcl3 as a strong lewis acid from industrial grade HCl and ordinary Al foil. I wanna know the yield ... |
8-10-2011 at 00:37
by: Adas |
Alcl3 synthesis
Two days ago a friend and I tried to make Aluminum Chloride.
We mixed bleach and fuming HCl to ge ... |
5-8-2011 at 19:29
by: Otter |
Making anhydrous Alcl3 - Al + HCl in polar aprotic solvent
I'm trying to think of a way to make anhydrous Alcl3 and all I can really think of is reacting Al with HCl in a polar aprotic solvent
like DMSO. If ... |
20-9-2010 at 11:44
by: cnidocyte |
Anhydrous Alcl3 attempt
... seeing chainhit's [url=http://www.sciencemadness.org/talk/viewthread.php?tid=14224]thread [/url] on Alcl3 with a barbeque I thought I'd
give it a try.
I used a Ca(OCl)2/HCl chlorine generator through ... |
24-8-2010 at 23:42
by: spong |
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