metalresearcher
National Hazard
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Registered: 7-9-2010
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Making CS2 from charcoal and sulfur ?
More than 10 years ago I prepared some CS2 vapor when I heated powdered charcoal and sulfur in a borosilicate test tube to red heat.
In the capturing glass I saw bubbling and it smelled like what is described as a smell of CS2.
I want to do this again : heating the mixture to red hot (600-800oC hotter is not possible as the borosilicate glass then melts like plastic) and
capturing it under water.
Does somebody have better ideas ?
I work in a well ventilated funehood because of the toxicity of CS2.
[Edited on 2011-4-16 by metalresearcher]
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entropy51
Gone, but not forgotten
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I sure do. Before starting a whole new thread, use the search engine.
It's quick and so easy that even lazy people can use it.
If you do, you will find existing threads like this one.
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metalresearcher
National Hazard
Posts: 731
Registered: 7-9-2010
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Mood: Reactive
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I have done before but couldn't find a suitable thread.
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Magpie
lab constructor
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Mood: Chemistry: the subtle science.
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see:
http://www.sciencemadness.org/talk/viewthread.php?tid=10564
The single most important condition for a successful synthesis is good mixing - Nicodem
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