clasienpharm
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Registered: 8-3-2006
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NEED HELP ON DATA ABOUT Diazotization of Cyclopropylamine
RED
I MEET DIFFICULTY TO DIAZOTIZATION Cyclopropylamine. if you are available for some data about this or who have some exp.about this reaction?
could you send me hand?
sd
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NERV
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Would you like my right or left hand  ?
Could you provide more information? Exactly what difficulties are you having, and what procedures are you using for the diazotization? We can’t
provide very much help without at least the basics of how you going about this, and what you have available.
Vir sapit qui pauca loquitur.
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clasienpharm
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Registered: 8-3-2006
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DIAZOTIZATION Cyclopropylamine,
I CAN'T GET CRYSTAL OF THE DIAZOTIZATION Cyclopropylamine,
Maybe the tri-ring have been spoilted!
Attachment: Doc1.doc (16kB)
This file has been downloaded 608 times
sd
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sparkgap
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"Maybe the tri-ring have been spoiled!"
Most likely. Diazotizing aliphatic amines usually result in the diazonium group leaving (favored entropy-wise due to the resultant gas release) and
the remaining carbocation reacting with anything in the environment. Given the lability of cyclopropane-containing compounds, a ring opening most
likely happened.
sparky (~_~)
"What's UTFSE? I keep hearing about it, but I can't be arsed to search for the answer..."
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