metalresearcher
National Hazard
Posts: 731
Registered: 7-9-2010
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Mood: Reactive
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Potassium mirror ?
Heating a question mark shaped retort tube which was welded on one end snd coupled with a 10mm borosilicate tube on the other end had a nice effect.
I heated K2CO3 + C to over 1200 C (probably more because the tube melted) and saw a nice mirror appearing on the glass tube. That must be condensed K
metal, but was unable to capture it in the oil. Anyway, after cooling I dismantled it and saw the still nice mirrored tube connected to the (deceased)
retort.
UPDATE: When it was cooled down I poured some water into the glass tube and indeed lilac flames appeared which was an indicator of the presence of K
metal.
[Edited on 2023-8-16 by metalresearcher]
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Johanson
Harmless
Posts: 39
Registered: 23-3-2023
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Dang nice! Would you mind showing us your heating arrangement/apparatus?
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Texium
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Thread Moved
30-11-2023 at 10:59 |
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