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Author: Subject: Bromination of Vanillin without bromine
Mailinmypocket
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[*] posted on 29-7-2013 at 06:23


Quote: Originally posted by turd  
Not to rain on your parade, but to qualify as real chemistry you have to provide some analytics - at least a mp.


Waiting on my capillary tubes from eBay... ;) I suppose I could try making my own but I'm not in that much of a rush. The post will be updated with the melting point when possible though!
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Mush
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[*] posted on 9-4-2015 at 17:13


AN ELEGANT AND COST -EFFECTIVE METHOD OF
AROMATIC BROMINATION USING SODIUM BROMIDE AND
HOUSEHOLD BLEACH

http://rasayanjournal.co.in/vol-5/issue-2/10.pdf

Vanillin entry 2, yield 80% 5-bromo-vanillin



A Multistep Synthesis Incorporating a Green Bromination of an Aromatic Ring
Pascal Cardinal, Brandon Greer, Horace Luong, and Yevgeniya Tyagunova
pp 1061–1063
Publication Date (Web): May 4, 2012 (Laboratory Experiment)
DOI: 10.1021/ed200579w



Attachment: A Multistep Synthesis Incorporating a Green Bromination.pdf (238kB)
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[Edited on 10-4-2015 by Mush]
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