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Vpatent357
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Hi Laboratory of Liptakov,
First, thank you for your research on new kit-explosives easy to do and your innovations.
Cyklonan 1 seems to be the easiest but is it powerful ? (good booster for example?)
And 300 mg of silver acetylide/nitrate primary are sufficient for the complete detonation of one cube? i don't have ETN,PETN,MHN...
For NC, ping-pong balls lacquer can be used?
Small blasting caps, fingers safe!
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Laboratory of Liptakov
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Hi Patent :-)
Ping pong balls? Sure, of course. In 90 g of acetone dissolved 10 g balls. Ag binary salt primer? Unfortunately, I do not know. Untested. But I
think, 300mg will be good kick. Or 0,2-0,3g HMTD, of course. Yes, Cyklonan (1 cube) is a good booster for AN /fuel/ Al mixture. Coming soon you see
Ammonium nitrate, special fuel without nitro esters composition on only primary 0,5g sensitive.
... ...LL
[Edited on 10-3-2015 by Laboratory of Liptakov]
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Vpatent357
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It remains for me to synthesize TACN
From what I know, it is secondary explosive. Is it safe to handle and store dry powder? more sensitive than ETN / PETN? for example
You have already experimented cyklonan with NC ping pong balls? it is of low quality and contains camphor ..
It's perfect I looking for exactly this kind of boost for AN mixtures, thank
I follow your youtube channel very closely
[Edited on 10-3-2015 by Vpatent357]
Small blasting caps, fingers safe!
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Laboratory of Liptakov
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Cyklonan 1 is similar sensitivity, low sensitivity as PETN. I see that Cyklonan works. Thank you for using Cyklonan explosive.......LL
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Trotsky
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Why would you use ping pong balls for a nitrocellulose source? I don't get how you've got silver acetylide, but have to resort to ping pong balls for
NC? Nitrocellulose is ridiculously easy to synthesize, everything you need to do it is readily available, just sulfuric acid, some nitrate salt, and
cotton balls, sodium carbonate or even bicarbonate to neutralize when you're finished. You don't have to watch the temp very close, if you make any
attempt at all to keep it cool you should have zero risk of runaway, especially with a small batch. And even if you have a runaway you're not at risk
of accidental explosion…
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Vpatent357
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Because I'm in the same approach as Dr. Liptakov,that is to say, Created my explosives as simply as possible with materials easily accessible and
without nitration ..
Yes SA.DS is very easy to do and effective as a primary, TACN seems very easy to produce secondary, even though we know nothing about him
(sensibility, storage..)
I can only find ammonia 20% and not 25%, it can work for the synthesis TACN? And are there specific recommendations for synthesis?
Small blasting caps, fingers safe!
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Laboratory of Liptakov
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Of course, only 20% NH3OH no problem to use. Because during the reaction concentration is decreasing. Perhaps 15%, perhaps only 10% at end of
reaction. That is no problem. The entire reaction works in a wide range. 10-40 g Cu wire. 50-120 g NH4NO3 dissolved. 100 -150 g NH3OH 15-25%. The
temperature reaction range 10-50 Celsius. 30 degrees Celsius is optimum, the optimum of 30 g of Cu, 100 g NH4NO3 optimum, 140 g NH3OH in aqa optimum
concentration of 20-25%. After cooling on 5C, separe on fine sieve. Dry. and etc. by Liptakov Channel.....LL
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PHILOU Zrealone
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Quote: Originally posted by Laboratory of Liptakov  | | Of course, only 20% NH3OH no problem to use. Because during the reaction concentration is decreasing. Perhaps 15%, perhaps only 10% at end of
reaction. That is no problem. The entire reaction works in a wide range. 10-40 g Cu wire. 50-120 g NH4NO3 dissolved. 100 -150 g NH3OH 15-25%. The
temperature reaction range 10-50 Celsius. 30 degrees Celsius is optimum, the optimum of 30 g of Cu, 100 g NH4NO3 optimum, 140 g NH3OH in aqa optimum
concentration of 20-25%. After cooling on 5C, separe on fine sieve. Dry. and etc. by Liptakov Channel.....LL |
NH4OH not NH3OH!
PH Z (PHILOU Zrealone)
"Physic is all what never works; Chemistry is all what stinks and explodes!"-"Life that deadly disease, sexually transmitted."(W.Allen)
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Laboratory of Liptakov
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Of course, NH4OH, thanks Philou, I'm sorry.... ......LL
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PHILOU Zrealone
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No problemo 
NH2OH (hydroxylamine) would be nice to experiment with owing to the high VOD of HAN (hydroxylamine nitrate - NH2OH.HNO3 (HO-NH3NO3)) (arround 8000
m/s).
I wonder if it will complexate competitively against NH3 via the NH2, via the OH or like NH2-NH2 with both.
[Edited on 14-3-2015 by PHILOU Zrealone]
PH Z (PHILOU Zrealone)
"Physic is all what never works; Chemistry is all what stinks and explodes!"-"Life that deadly disease, sexually transmitted."(W.Allen)
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Marcello0922
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| Quote: Originally posted by Rosco Bodine | @ LL I agree about the possibility of a mixed salt of TACN and TACP being the product. A synthesis of TACP which I described many years ago and
posted again recently uses Cu(NO3)2 as precursor for TACP, however the yield resulting is lower than what would be quantitative for the desired TACP.
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If you are synthesizing TACP using Cu(NO3)2 then the final reaction produces about 90% TACP and 10% TACN - I have tested this several times using XRD.
Synthesis of TACP with NH4ClO4, CuO and NH3(aq) gives a pure product. XRD showed that [Cu(NH3)4](ClO4)2 is then formed as a deformed octahedron.
The most interesting thing is that with the above method and the addition of hexamine, the reaction proceeds even at room temperature (reaction
catalyst?), while the XRD products showed that:
[Cu(NH3)5][NH3](ClO4)3 - crystals in the form of a pyramid with a square base and a perfect trigonal bipyramid. The content of the latter compound was
about 86%, while [Cu(NH3)4](ClO4)2 was only 14%.
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Etanol
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| Quote: Originally posted by Marcello0922 |
The most interesting thing is that with the above method and the addition of hexamine, the reaction proceeds even at room temperature (reaction
catalyst?), while the XRD products showed that:
[Cu(NH3)5][NH3](ClO4)3 - crystals in the form of a pyramid with a square base and a perfect trigonal bipyramid. The content of the latter compound was
about 86%, while [Cu(NH3)4](ClO4)2 was only 14%. |
[Cu(NH3)5][NH3](ClO4)3 ?
Copper(III) complex?
May be [Cu(NH3)5][NH4](ClO4)3 or [Cu(NH3)4][NH4](ClO4)3 ?
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Marcello0922
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The pattern I wrote was confirmed by 3 people - 1 who did the XRD study and 2 who do the spectra resolving. And this was on 5 samples after each
synthesis. I know this is strange.
But I have another question by the way: what products can be in the filtrate? In addition to the Schweizer reagent, of course. And unreacted hexamine
or ammonium perchlorate.
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Laboratory of Liptakov
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Interesting research of crystalography, Marcello.....With a lot pyamides.
In mother liquor will NH4ClO4, CuO, diluted TACP, diluted hexamine + ammmonium hydroxide. This liquor
is possible evaporate about cca 30 C and obtain next dry energetic material with different (usually slow burned) properties against TACP / CHP.
Mother liquor 10g + 100g dH2O is also possible boil at cca 100 C.
At the high temperature arise fine dry powder CuO, crystalls NH4ClO4+ crystalls hexamine. All gas NH3/4 get out from solution.
At boiling pure TACP mother liquor arise CuO powder + NH4ClO4. All gas NH3/4 get out from solution....
Development of primarily - secondary substances CHP (2015) Lithex (2022) Brightelite (2023) Nitrocelite and KC primer (2024)
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