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Author: Subject: residual solvent
mansi2005
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[*] posted on 17-5-2006 at 01:32
residual solvent


In our API IPA as a residual solvent appear as 9000 ppm limit is 2000 ppm & drying condition is 80°C under vaccum. so how can i remove it? please suggest me appropriate answer.
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stoichiometric_steve
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[*] posted on 17-5-2006 at 02:37


calcium chloride.
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bio2
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[*] posted on 17-5-2006 at 03:05


IPA doesn't react as readily as lower alcohols with CaCl2

.........drying condition is 80°C under vaccum.........

With a rotary evaporator?

Need details like how long at what pressure etc.
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Aboveneh
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[*] posted on 17-5-2006 at 03:25
Drying your subustance with P2O5


guys have u ever done drying your subustance with P2O5 , can some body post details , including setup of instrumetnts. Help apperciated .
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