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Author: Subject: Na-DCCA for Chlorobenzene
DFliyerz
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[*] posted on 30-11-2015 at 09:17
Na-DCCA for Chlorobenzene


I saw a preparation of chlorobenzene using TCCA and 50% sulfuric acid in the documentation for the preparation of pentryl; would I be correct in assuming that Na-DCCA would work if the amounts were compensated?
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Boffis
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[*] posted on 2-12-2015 at 07:36


You will probably need to use more sulphuric acid and less water to compensate for the tendency of the sodium salt to neutralise part of the acid. Plus 50% more Na-DCCA (molar terms) than TCCA. Let us know how you get on please. :)
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