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Author: Subject: Can't figure out synthesis
draculic acid69
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[*] posted on 6-3-2023 at 01:34


Quote: Originally posted by blogfast25  
Quote: Originally posted by draculic acid69  


CBD or ethanol extract is dissolved in ethanol, concentrated, acidified, refluxed
then neutralize with excess aqueous bicarbonate solution then extract with
toluene,seperate and evaporate


Ok, thanks. And what acid is proposed: higher up p-toluenesulfonic acid was mentioned?


A few drops of sulfuric in ethanol is sufficient
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draculic acid69
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[*] posted on 6-3-2023 at 01:42


Quote: Originally posted by Ephraim_Bane  
If you just want to make some cheap THC, then *any* acid will work fine. A standard thing people do as kitchen chemistry is to microwave a solution of citric acid and CBD in water.


I doubt any acid works. Gaa doesnt make any noticeable change so I doubt citric will do anything
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blogfast25
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[*] posted on 6-3-2023 at 03:53


Quote: Originally posted by draculic acid69  

A few drops of sulfuric in ethanol is sufficient


Ok, once the CBD is succesfully converted to delta-8, how to work up? That is, how to seperate and obtain the product?




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[*] posted on 6-3-2023 at 08:24


Quote: Originally posted by blogfast25  
The papers are paywalled, so I can't read them.
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